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3. CLA ethyl ester �젣議�
Alkali 珥됰ℓ濡� �빀�꽦�맂 CLA 利� 吏�諛⑹궛 �삎�깭瑜� ethyl ester �삎�깭濡� �쟾�솚�븯湲� �쐞�븯�뿬 2%臾댁닔�솴�궛-�뿉������濡� 媛��븯�뿬 �빟 20遺꾧컙 �솚瑜섎컲�쓳 �떆�궓 �썑 n-Hexane�쓣 �씠�슜�븯�뿬 CLA ethyl ester瑜� �쉶�닔�븯���怨� �쉶�쟾吏꾧났 利앸컻湲곕�� �씠�슜�븯�뿬 n-Hexane�쓣 �젣嫄고븯����떎.
4. Urea adduct瑜� �씠�슜�븳 CLA �냽異�
�빐諛붾씪湲곗뵪�쑀濡쒕���꽣 alkali 珥됰ℓ瑜� �씠�슜�븯�뿬 �빀�꽦�맂 CLA(吏�諛⑹궛�삎�깭)��� CLA ethyl ester �삎�깭 利� �몢媛�吏� �삎�깭濡� �굹�늻�뼱 �떆�룄�릺�뿀�쑝硫� �씠�븣 �궗�슜�맂 �슜留ㅻ줈�뒗 �뿉������怨� 硫뷀����� �몢媛�吏��쓽 �슜留ㅺ�� �떆�룄�릺�뿀�떎. 洹� 怨쇱젙��� �떎�쓬怨� 媛숇떎. �떆猷�(CLA��� CLA ethyl ester)�뿉 ����븯�뿬 urea瑜� 0.5諛� - 4.0諛곗쓽 urea瑜� 媛��븯怨� �씪�젙�웾�쓽 �슜留�(�뿉������ �삉�뒗 硫뷀�����)瑜� 媛��븳�썑 urea媛� �셿�쟾�엳 �슜�빐�릺湲곌퉴吏� magnetic stirrer�뿉�꽌 援먮컲�븯硫댁꽌 媛��뿴�븯����떎. urea媛� �셿�쟾�엳 �슜�빐�맂�썑�뿉�뒗 �솚瑜섎깋媛곴���뿉�꽌 遺꾨━�븳 �썑 �떎�삩�뿉�꽌 30 -40遺꾧컙 �깋媛곹븯怨� �떎�떆 4�꼦�뿉�꽌 24�떆媛꾨룞�븞 諛⑹튂�븯����떎. 媛먯븬�뿬怨쇨린瑜� �씠�슜�븯�뿬 寃곗젙�솕�맂 urea瑜� �젣嫄고븯怨� �궓��� �븸�긽遺�遺�(硫뷀����� �삉�뒗 �뿉������) 利� Non urea adduct 遺꾪쉷�쓣 �쉶�닔�븳 �썑 0.1N HCl �닔�슜�븸�쓣 媛��븯怨� �떎�떆 n-Hexane�쓣 媛��븯�뿬 urea�뿉 adduct�릺吏� �븡��� 遺꾪쉷�쓣 n-Hexane 痢듭쑝濡쒕���꽣 �쉶�닔�븯����떎.
5. 珥덉엫怨� �씠�궛�솕�깂�냼瑜� �씠�슜�븳 CLA ethyl ester�쓽 �젙�젣
蹂� �뿰援ъ떎�뿉�꽌 �젣�옉�븳 珥덉엫怨� �씠�궛�솕�깂�냼 異붿텧�옣移섎�� �씠�슜�븯�뿬 CLA ethyl ester濡쒕���꽣 �궛�솕臾쇱쓣 �젣嫄고븯湲� �쐞�븳 �젙�젣議곌굔�쓣 議곗궗�븯�뿬 蹂댁븯�떎. 異붿텧怨쇱젙以묒쓽 �삩�룄議곌굔��� 媛��옣 �궙��� �삩�룄議곌굔�씤 40�꼦瑜� �꽕�젙�븯����쑝硫� �븬�젰議곌굔��� 2500 psi, 2000 psi, 1500 psi�벑 3媛�吏� �븬�젰議곌굔蹂꾨줈 異붿텧�떎�뿕�쓣 �떎�떆�븯�뿬 CLA ethyl ester�쓽 �슜�빐�룄 諛� 媛� 遺꾪쉷�쓽 �궛�솕臾쇱쓽 異붿텧�젙�룄瑜� 鍮꾧탳�븯�뿬 蹂댁븯�떎. �씠�븣���(�깮�왂)
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1. Comparision of methylation methods for the quantitation of conjugated Linoleic Acid isomers. 1993. N. C. Shantha, E. A. Eecker, and B. Hennig. J. AOAC, 76:644節�649
2. Determination of conjugated linoleic acid content and isomer distribution in three cheddar-type cheese : Effects of cheese cultures, processing, and aging. 1992. S. A. Werner, L. O. Luedecke, and T. D. Shultz. J. Agric. Food. Chem., 40: 1817節�1821
3. Preparation of geometrical isomers of linolenic acid. 1987. A. Grandgirard, F. Julliard, J. Prevost and J. R. Sebedio. J. AOAC. 64: 1434節�
4. Fractionation of cis- and trans-oleic, linoleic, and conjugated linoleic fatty acid methyl esters by silver ion high-performance liquid chromatography.1998. R. Adlof, and T. Lamm. J. Chromatography A. 799:329節�332
5. Analysis of fatty acid mono- and diacylglycerol positional isomers by silver ion high-performance liquid chromatography. 1996. R. O. Adlof, J. Chromatography A. 741:135節�138
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�쓽 �냽異� 諛� �젙�젣_hwp_01_.gif "Conjugated Linoleic Acid(CLA)�쓽 �냽異� 諛� �젙�젣 (1 페이지)")
�쓽 �냽異� 諛� �젙�젣_hwp_02_.gif "Conjugated Linoleic Acid(CLA)�쓽 �냽異� 諛� �젙�젣 (2 페이지)")
�쓽 �냽異� 諛� �젙�젣_hwp_03_.gif "Conjugated Linoleic Acid(CLA)�쓽 �냽異� 諛� �젙�젣 (3 페이지)")
�쓽 �냽異� 諛� �젙�젣_hwp_04_.gif "Conjugated Linoleic Acid(CLA)�쓽 �냽異� 諛� �젙�젣 (4 페이지)")
�쓽 �냽異� 諛� �젙�젣_hwp_05_.gif "Conjugated Linoleic Acid(CLA)�쓽 �냽異� 諛� �젙�젣 (5 페이지)")
�쓽 �냽異� 諛� �젙�젣_hwp_01.gif "Conjugated Linoleic Acid(CLA)�쓽 �냽異� 諛� �젙�젣 (1 페이지)")
�쓽 �냽異� 諛� �젙�젣_hwp_02.gif "Conjugated Linoleic Acid(CLA)�쓽 �냽異� 諛� �젙�젣 (2 페이지)")
�쓽 �냽異� 諛� �젙�젣_hwp_03.gif "Conjugated Linoleic Acid(CLA)�쓽 �냽異� 諛� �젙�젣 (3 페이지)")
�쓽 �냽異� 諛� �젙�젣_hwp_04.gif "Conjugated Linoleic Acid(CLA)�쓽 �냽異� 諛� �젙�젣 (4 페이지)")
�쓽 �냽異� 諛� �젙�젣_hwp_05.gif "Conjugated Linoleic Acid(CLA)�쓽 �냽異� 諛� �젙�젣 (5 페이지)")
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